Nickel in PDB 4m4m: The Structure of Ni T6 Bovine Insulin

The structure of The Structure of Ni T6 Bovine Insulin, PDB code: 4m4m was solved by C.G.Frankaer, P.Harris, K.Stahl, with X-Ray Crystallography technique. A brief refinement statistics is given in the table below:

Resolution Low / High (Å)	16.78 / 1.50
Space group	H 3
Cell size a, b, c (Å), α, β, γ (°)	80.850, 80.850, 33.360, 90.00, 90.00, 120.00
R / Rfree (%)	18.2 / 22.4

The binding sites of Nickel atom in the The Structure of Ni T6 Bovine Insulin (pdb code 4m4m). This binding sites where shown within 5.0 Angstroms radius around Nickel atom.
In total 2 binding sites of Nickel where determined in the The Structure of Ni T6 Bovine Insulin, PDB code: 4m4m:
Jump to Nickel binding site number: 1; 2;

Nickel binding site 1 out of 2 in the The Structure of Ni T6 Bovine Insulin


Mono view


Stereo pair view

A full contact list of Nickel with other atoms in the Ni binding site number 1 of The Structure of Ni T6 Bovine Insulin within 5.0Å range: probe atom residue distance (Å) B Occ B:Ni101 b:13.2 occ:0.33 NE2 B:HIS10 2.1 12.7 1.0 O B:HOH201 2.1 17.8 1.0 CE1 B:HIS10 3.1 19.7 1.0 CD2 B:HIS10 3.1 10.7 1.0 HE1 B:HIS10 3.2 23.6 1.0 HD2 B:HIS10 3.3 12.8 1.0 O B:HOH223 3.7 34.3 1.0 ND1 B:HIS10 4.2 20.5 1.0 CG B:HIS10 4.2 14.7 1.0 HD1 B:HIS10 5.0 24.5 1.0

Nickel binding site 2 out of 2 in the The Structure of Ni T6 Bovine Insulin


Mono view


Stereo pair view

A full contact list of Nickel with other atoms in the Ni binding site number 2 of The Structure of Ni T6 Bovine Insulin within 5.0Å range: probe atom residue distance (Å) B Occ D:Ni101 b:14.7 occ:0.33 NE2 D:HIS10 2.0 18.6 1.0 O D:HOH201 2.2 27.0 1.0 CE1 D:HIS10 3.0 22.1 1.0 CD2 D:HIS10 3.1 15.7 1.0 HE1 D:HIS10 3.1 26.5 1.0 O D:HOH220 3.2 58.2 0.3 HD2 D:HIS10 3.3 18.7 1.0 O D:HOH219 4.0 47.1 1.0 ND1 D:HIS10 4.1 20.1 1.0 CG D:HIS10 4.2 15.4 1.0 O D:HOH212 4.6 30.0 1.0 HD1 D:HIS10 4.9 24.1 1.0

C.G.Frankaer, S.Mossin, K.Stahl, P.Harris. Towards Accurate Structural Characterization of Metal Centres in Protein Crystals: the Structures of Ni and Cu T6 Bovine Insulin Derivatives. Acta Crystallogr.,Sect.D V. 70 110 2014.
ISSN: ISSN 0907-4449
PubMed: 24419384
DOI: 10.1107/S1399004713029040