Nickel in PDB 3nv4: Crystal Structure of Human Galectin-9 C-Terminal Crd in Complex with Sialyllactose

The structure of Crystal Structure of Human Galectin-9 C-Terminal Crd in Complex with Sialyllactose, PDB code: 3nv4 was solved by H.Yoshida, S.Kamitori, with X-Ray Crystallography technique. A brief refinement statistics is given in the table below:

Resolution Low / High (Å)	30.64 / 1.99
Space group	P 63
Cell size a, b, c (Å), α, β, γ (°)	70.766, 70.766, 50.480, 90.00, 90.00, 120.00
R / Rfree (%)	18.3 / 22.6

The binding sites of Nickel atom in the Crystal Structure of Human Galectin-9 C-Terminal Crd in Complex with Sialyllactose (pdb code 3nv4). This binding sites where shown within 5.0 Angstroms radius around Nickel atom.
In total only one binding site of Nickel was determined in the Crystal Structure of Human Galectin-9 C-Terminal Crd in Complex with Sialyllactose, PDB code: 3nv4:

Nickel binding site 1 out of 1 in the Crystal Structure of Human Galectin-9 C-Terminal Crd in Complex with Sialyllactose


Mono view


Stereo pair view

A full contact list of Nickel with other atoms in the Ni binding site number 1 of Crystal Structure of Human Galectin-9 C-Terminal Crd in Complex with Sialyllactose within 5.0Å range: probe atom residue distance (Å) B Occ A:Ni401 b:20.4 occ:0.50 O A:HOH12 2.1 18.2 1.0 NE2 A:HIS320 2.2 22.7 1.0 CD2 A:HIS320 3.0 20.5 1.0 CE1 A:HIS320 3.3 21.7 1.0 O A:VAL321 4.2 21.9 1.0 CG A:HIS320 4.2 23.1 1.0 ND1 A:HIS320 4.3 19.3 1.0 OH A:TYR191 4.7 25.2 1.0

H.Yoshida, M.Teraoka, N.Nishi, S.Nakakita, T.Nakamura, M.Hirashima, S.Kamitori. X-Ray Structures of Human Galectin-9 C-Terminal Domain in Complexes with A Biantennary Oligosaccharide and Sialyllactose J.Biol.Chem. V. 285 36969 2010.
ISSN: ISSN 0021-9258
PubMed: 20861009
DOI: 10.1074/JBC.M110.163402